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2018

Metal-free class Ie ribonucleotide reductase from pathogens initiates catalysis with a tyrosine-derived dihydroxyphenylalanine radical, E. J. Blaesi, Palowitch, G. M., Hu, K., Kim, A. J., Rose, H. R., Alapati, R., Lougee, M. G., Kim, H. Jong, Taguchi, A. T., Tan, K. Ooi, Laremore, T. N., Griffin, R. G., Krebs, C., Matthes, M. L., Silakov, A., J. Jr., M. Bollinger, Allen, B. D., and Boal, A. K., , Proceedings of the National Academy of Sciences, vol. 115, pp. 10022–10027, 2018.

Overhauser effects in non-conducting solids at 1.2 K, X. Ji, Can, T. V., Mentink-Vigier, F., Bornet, A., Milani, J., Vuichoud, B., Caporini, M. A., Griffin, R. G., Jannin, S., Goldman, M., and Bodenhausen, G., , Journal of Magnetic Resonance, vol. 286, pp. 138 - 142, 2018.

Primary Transfer Step in the Light-Driven Ion Pump Bacteriorhodopsin: An Irreversible U-Turn Revealed by Dynamic Nuclear Polarization-Enhanced Magic Angle Spinning NMR, Q. Zhe Ni, Can, T. V., Daviso, E., Belenky, M., Griffin, R. G., and Herzfeld, J., , Journal of the American Chemical Society, vol. 140, no. 11, pp. 4085 - 4091, 2018.

The structure of a β2-microglobulin fibril suggests a molecular basis for its amyloid polymorphism, M. G. Iadanza, Silvers, R., Boardman, J., Smith, H. I., Karamanos, T. K., Debelouchina, G. T., Su, Y., Griffin, R. G., Ranson, N. A., and Radford, S. E., , Nature Communications, vol. 9, 2018.

2017

17O MAS NMR Correlation Spectroscopy at High Magnetic Fields, E. G. Keeler, Michaelis, V. K., Colvin, M. T., Hung, I., Gor’kov, P. L., Cross, T. A., Gan, Z., and Griffin, R. G., , Journal of the American Chemical Society, vol. 139, pp. 17953-17963, 2017.

3D MAS NMR Experiment Utilizing Through-Space 15N–15N Correlations, K. J. Donovan, Silvers, R., Linse, S., and Griffin, R. G., , Journal of the American Chemical Society, vol. 139, pp. 6518–6521, 2017.

Aggregation and Fibril Structure of AβM01-42 and Aβ1-42, R. Silvers, Colvin, M. T., Frederick, K. K., Jacavone, A. C., Lindquist, S. L., Linse, S., and Griffin, R. G., , Biochemistry, vol. 56, no. 36, pp. 4850-4859, 2017.

Combining DNP NMR with segmental and specific labeling to study a yeast prion protein strain that is not parallel in-register, K. K. Frederick, Michaelis, V. K., Caporini, M. A., Andreas, L. B., Debelouchina, G. T., Griffin, R. G., and Lindquist, S., , Proceedings of the National Academy of Sciences, vol. 114, pp. 3642–3647, 2017.

Frequency-Swept Integrated Solid Effect, T. V. Can, Weber, R. T., Walish, J. J., Swager, T. M., and Griffin, R. G., , Angewandte Chemie International Edition, vol. 56, pp. 6744–6748, 2017.

In-Situ Characterization of Pharmaceutical Formulations by Dynamic Nuclear Polarization Enhanced MAS NMR, Q. Zhe Ni, Yang, F., Can, T. V., Sergeyev, I. V., D’Addio, S. M., Jawla, S. K., Li, Y., Lipert, M. P., Xu, W., Williamson, R. Thomas, Leone, A., Griffin, R. G., and Su, Y., , The Journal of Physical Chemistry B, vol. 121, no. 34, pp. 8132-8141, 2017.

Off-resonance NOVEL, S. K. Jain, Mathies, G., and Griffin, R. G., , The Journal of Chemical Physics, vol. 147, p. 164201, 2017.

Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR, Q. Zhe Ni, Markhasin, E., Can, T. V., Corzilius, B., Tan, K. Ooi, Barnes, A. B., Daviso, E., Su, Y., Herzfeld, J., and Griffin, R. G., , The Journal of Physical Chemistry B, vol. 121, pp. 4997–5006, 2017.

Proton-Assisted Recoupling (PAR) in Peptides and Proteins, K. J. Donovan, Jain, S. K., Silvers, R., Linse, S., and Griffin, R. G., , The Journal of Physical Chemistry B, vol. 121, pp. 10804-10817, 2017.

Ramped-amplitude NOVEL, T. V. Can, Weber, R. T., Walish, J. J., Swager, T. M., and Griffin, R. G., , The Journal of Chemical Physics, vol. 146, p. 154204, 2017.

2016

17O NMR Investigation of Water Structure and Dynamics, E. G. Keeler, Michaelis, V. K., and Griffin, R. G., , The Journal of Physical Chemistry B, vol. 120, pp. 7851–7858, 2016.

Atomic Resolution Structure of Monomorphic Aβ42Amyloid Fibrils, M. T. Colvin, Silvers, R., Ni, Q. Zhe, Can, T. V., Sergeyev, I., Rosay, M., Donovan, K. J., Michael, B., Wall, J., Linse, S., and al., et, , Journal of the American Chemical Society, vol. 138, pp. 9663–9674, 2016.

Gd(iii) and Mn(ii) complexes for dynamic nuclear polarization: small molecular chelate polarizing agents and applications with site-directed spin labeling of proteins, M. Kaushik, Bahrenberg, T., Can, T. V., Caporini, M. A., Silvers, R., Heiliger, J., Smith, A. A., Schwalbe, H., Griffin, R. G., and Corzilius, B., , Phys. Chem. Chem. Phys., vol. 18, pp. 27205–27218, 2016.

Polymer Structure Dependent Hierarchy in PolyMOC Gels, A. V. Zhukhovitskiy, Zhao, J., Zhong, M., Keeler, E. G., Alt, E. A., Teichen, P., Griffin, R. G., Hore, M. J. A., Willard, A. P., and Johnson, J. A., , Macromolecules, vol. 49, pp. 6896–6902, 2016.

Pulsed Dynamic Nuclear Polarization with Trityl Radicals, G. Mathies, Jain, S., Reese, M., and Griffin, R. G., , The Journal of Physical Chemistry Letters, vol. 7, pp. 111–116, 2016.

Star PolyMOCs with Diverse Structures, Dynamics, and Functions by Three-Component Assembly, Y. Wang, Gu, Y., Keeler, E. G., Park, J. V., Griffin, R. G., and Johnson, J. A., , Angewandte Chemie, vol. 129, pp. 194–198, 2016.

2015

Biosilica-Entrapped Enzymes Studied by Using Dynamic Nuclear-Polarization-Enhanced High-Field NMR Spectroscopy, E. Ravera, Michaelis, V. K., Ong, T. - C., Keeler, E. G., Martelli, T., Fragai, M., Griffin, R. G., and Luchinat, C., , ChemPhysChem, vol. 16, pp. 2751–2754, 2015.

Dynamic DMF Binding in MOF-5 Enables the Formation of Metastable Cobalt-Substituted MOF-5 Analogues, C. K. Brozek, Michaelis, V. K., Ong, T. - C., Bellarosa, L., López, N., Griffin, R. G., and Dincă, M., , ACS Central Science, vol. 1, pp. 252–260, 2015.

Efficient Dynamic Nuclear Polarization at 800 MHz/527 GHz with Trityl-Nitroxide Biradicals, G. Mathies, Caporini, M. A., Michaelis, V. K., Liu, Y., Hu, K. - N., Mance, D., Zweier, J. L., Rosay, M., Baldus, M., and Griffin, R. G., , Angewandte Chemie International Edition, vol. 54, pp. 11770–11774, 2015.

High Resolution Structural Characterization of Aβ42Amyloid Fibrils by Magic Angle Spinning NMR, M. T. Colvin, Silvers, R., Frohm, B., Su, Y., Linse, S., and Griffin, R. G., , Journal of the American Chemical Society, vol. 137, pp. 7509–7518, 2015.

Highly branched and loop-rich gels via formation of metal–organic cages linked by polymers, A. V. Zhukhovitskiy, Zhong, M., Keeler, E. G., Michaelis, V. K., Sun, J. E. P., Hore, M. J. A., Pochan, D. J., Griffin, R. G., Willard, A. P., and Johnson, J. A., , Nature Chemistry, vol. 8, pp. 33–41, 2015.

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